last updated Wednesday, September 17, 2008

Arrhenius equation predicts that the rate of reaction increases if the temperature is raised
Aspirator is a device that produces vacuum by means of the Venturi effect. In an aspirator, fluid (liquid or gaseous) flows through a tube which then narrows. When the tube narrows, the fluid's speed increases, and because of the Venturi effect, its pressure decreases. Vacuum is taken from this point
Atropisomer is a stereoisomer that results from hindered rotation about a single bond where the steric strain barrier to rotate is high enough to isolate the different conformers.
Beer-Lambert-Law is the basic law for all absorption processes (A=ecl). It states that the absorbance of a sample is directly proportional to the concentration of the solute in the sample, the pathlength and the molar extinction coefficient (e). The law only applies for very diluted solution (<10-4 mol/L).
Bathochromic shift is a shift to higher wavelength in the UV-Vis spectrum
Boiling point is the temperature when a liquid becomes a gas. It depends highly on the surrounding pressure
Catalyst is a compound that increases the rate of the reaction by lowering the activation energy for a chemical reaction, but does not change the yiel
Chromatography is a technique to separate compounds from each other. It is based on the distribution various compounds between the mobile phase (see below) and the stationary phase (see below).
Chromophore is a chemical group that absorbs light at a specific wavelength and so imparts color to a molecule i.e. carbonyl group or azo group
Condensation point is the temperature at which the conversion of a substance from the vapor state to a denser liquid or solid state takes place usually initiated by a reduction in temperature of the vapor
Coupling constant characterizes the line spacing within a multiplet in a 1H-NMR spectrum, which permits conclusions about the distance and the angle of interaction of the coupling partners
Decant(ing) the process in the laboratory when a liquid is transferred into a different container and the solid is left behind
Dew point

the temperature at which a vapor begins to condense (which is not equal to the boiling point!)

Diastereomer is a stereoisomer of a compound having two or more chiral centers that is not a mirror image of another stereoisomer of the same compound i.e borneol and isoborneol
Disproportionation refers to the transformation of a substance into two or more dissimilar substances usually by simultaneous oxidation and reduction i.e. Mn(III) forms Mn(II) and Mn(IV).
Distillation is a technique to purify liquids based on different boiling points
Distribution coefficent also called partition coefficient. Quantifies the distribution of a compound between two different phases (K=c1/c2)
Emulsion is a suspension of finely divided particles in a continuous medium in which the particles are approximately 5 to 5,000 Å in size, do not settle out of the substance rapidly, and are not readily filtered i.e. oil and vinegar in a vinegrette, or fat in water in milk
Enantiomer is a molecule that is not superimposable on its mirror image, related to chirality
Enantiomeric excess is the ratio of one enantiomer to the other enantiomer in a mixture (abbreviated: e.e. or ee). It is often used in context of asymmetric synthesis. Related: diastereomeric excess.
Exclusion rule describes the fact that a molecule with a center of inversion has peaks either in the IR or in the Raman spectrum, but not in both.
Extraction is a process to isolate a compound from a mixture by either temporary chemical modification or distribution within two layers.
FID =Flame Ionization Detector, a detector used in GC chromatography, very sensitive but destroys the sample due to combustion
Freezing point is the temperature at which a liquid becomes a solid. Its depression can be used to determine the molecular weight of compounds (=collagative property)
Hammond Postulate If two states, as for example, a transition state and an unstable intermediate, occur consecutively during a reaction process and have nearly the same energy content, their interconversion will involve only a small reorganization of the molecular structures. That is, along the reaction coordinate, species with similar energies also have similar structures
Heterogeneous is a system that consists of at least two phases (solid-liquid)
Homogeneous is a system that consists of only one phase i.e. solution
HOMO is the highest occupied molecular orbital in a molecule
Hygroscopic is a compound that absorbs water from the air or a solution, nature of drying agents
Hyperchromic Increased absorption of UV-Vis light (opposite: hypochromic)
Hypsochromic shift is the shift to lower wavelength in the UV-Vis spectrum (opposite: bathochromic)
In-situ refers to the synthesis of a reactive intermediate, which is not isolated since it is too difficult or too dangerou
Infrared spectroscopy is a spectroscopic technique to identify functional groups, looks at vibrational modes of the molecule. The modern instruments are FTIR instruments.
Lachrymator a compound that makes the eyes fill with tears but does not damage them (“teargas”)
Le Châtelier Principle describes equilibrium reactions and how to influence them
Lock-and-Key method describes the selectivity of enzymes towards certain substrates over others
LUMO lowest unoccupied molecular orbital
Melting point is the temperature at which a solid becomes a liquid, usually reported as a range
Metallorganic a compound that possesses carbon but no direct M-C bond i.e. sodium acetate
Methylene chloride =dichloromethane
Mobile phase is a term used in chromatography. It consists usually of an organic solvent (or mixture) in column chromatography
Mother liquor the solution that was separated from the crystals
Neat a term often used in IR spectroscopy, means that only the pure compound was place in the IR beam
NMR spectroscopy is a spectroscopic technique to identify functional groups and structure of a compound. It looks at behavior of nuclear spins in an external magnetic field, frequently used as 1H or 13C-NMR spectroscopy in organic laboratories
Oligomer is a polymer or polymer intermediate containing relatively few structural units (more than two units) i.e. dimer, trimer
Organometallic the compound has at least one metal-carbon bond i.e. Grignard reagent, ferrocene, etc
Petroleum ether (also called Petrolether or ligroin) is a mixture of different hydrocarbons. The name does not refer to oxygen containing compounds but much more on its volatility
Pyrolysis is the process where organic compounds decompose when heated without burning.
Pyrophoric means that a compound catches on fire when it comes in contact with air. Many finely divided metal powder or strong reducing reagents react like this i.e. Raney Nickel, LiAlH4
PTC =Phase Transfer Catalysis, utilizes a catalyst which is able to transport an ion from one phase (usually aqueous) into the other phase (organic).
Quenching a reaction is terminating by deactivating reactive intermediates
Racemic a mixture that is composed of equal amounts of dextrorotatory and levorotatory forms of the same compound and is not optically active
Recrystallization is a technique used to purify solids based on different solubilities of the impurity and the target compound.
Reflux implies that a solution/solvent is heated to a boil while maintaining its volume constant. This is usually accomplished by using a device to catch the solvent vapors i.e. condenser
Refractive Index is a physical property that quantifies the refraction of light by a solid or liquid. It highly depends on the temperature and the wavelength it is observed
Retardation factor is the ratio of how far the center of a spot traveled compared to the solvent front (=Rf-value)
Retention time is the time interval that passed between the sample injection and the appearance of the peak maximum
Rinsing/Rinse refers to the washing of a solid with small amounts of cold solvent to remove mother liquor and impuries from the surface
Saturated solution is a solution that contains the maximum amount of solute at a given temperature.
Seeding is a technique to initiate crystallization from saturated or super-saturated solutions
Split-mode refers to the fact that only a small amount of the sample is actually introduced to the GC column
Stationary phase is a term used in chromatography. It refers to the part, which absorbs the compound. The stronger the interaction is, the longer the compound requires moving through the column
Sublimation point is the temperature at which a solid evaporates without melting first
Superheating the process at which a liquid is heated above its boiling point without vaporization. Can be avoided by adding boiling stones, boiling sticks or a spin vane
Supersaturated is a solution that contains more than the maximum amount of solute at a given temperature. Often causes problems during the recrystallization process.
TCD =Thermal Conductivity Detector, less sensitive than FID, but allows to collect sample
Trituration commonly refers to the grinding of powders in a pestle or mortar. It is a method to induce crystallization of a pure compound from an impure oil or the process of separating two solids by selectively dissolving one compound while the other is insoluble.
UV-Vis spectroscopy is a technique to investigate conjugation within molecules. Often used for colored compounds. Looks at the excitation of electrons from a bonding to an anti-bonding orbital
Vacuum filtration is a filtration technique that permits to separate a solid from a liquid. The vacuum increases the flow rate of the mother liquor through the filter paper. Not suitable for low boiling or hot solvents!
Washing is a process to remove small amounts of byproducts or a catalyst from a reaction mixture.
Zaitsev Rule predicts the formation of an alkene based on thermodynamic stability: the alkene with the highest the degree of substitution is preferentially formed under thermodynamic conditions.